SKU
R50-Unistat405-UDP6

Crystallization and Isolation Package - Ai 50L Glass Reactor

Price $49,725.00

CUSTOMIZE YOUR PRODUCT

Wishlist

Product Video

Videos

Ai R-series single/dual jacketed glass reactors are designed for synthetic reaction of different types of materials in a controlled temperature and vacuum environment. Each reactor features adjustable stirring speeds and a constant pressure feeding funnel that allows you to add material to the vessel at a uniform and controlled speed. The built-in condenser makes it possible to recover some materials, also at a controlled rate of speed.

Features

  • Now includes a FREE high quality thermo insulation jacket (a $699 value) with open/close viewing window and top/bottom adjustable drawstrings, specially designed and made for Ai glass jacketed reactors. These jackets will extend chiller life, allow you to go down to a lower temperature, and also cut your utility bill.
  • Dual jacketed model allows you to draw vacuum from the outer jacket, thus protects your recirculating fluid temperature and gives you best control over your work. It also help prevents frost to form on the outside of the vessel, allowing you to see clearly into your material.
  • Solvent-resistant PTFE on all sealing components ensures long time durability and operation.
  • All glassware is hand-made from food grade high borosilicate glass that is heat/cold/corrosion-resistant.
  • Adjustable stirring rate provides great torque or high speed.
  • Patented PTFE stirring rod bearing for reliable and quiet operation.
  • Optional multi-layer stirring blades for optimal reaction results.
  • Wide range of temperature operations, from -110F to 400F.
  • Large condenser cooling surface for exceptional condensation performance.
  • Rugged stainless steel reinforced PTFE stirrer with anchored agitator, suitable for a wide range of viscous materials.
  • Easily visual operation with digital speed and temperature displays.
  • Heavy duty stainless steel supporting framework with lockable casters for mobility and stability. (whole support and glass vessel shipped pre-assembled)
  • One year warranty and lifetime US-based parts, service, and support.

Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

 

 

Specifications

Specifications

Model R50
Electrical requirements
110V 60Hz or 220V 50/60Hz, 1-Phase, 140W
Reaction glass vessel capacity
13 gallons (50L)
Cooling/heating jacket capacity
4.2 gallons (16L)
Glass material High borosilicate glass 3.3
Rotation controller Digital controller with variable frequency drive
Rotation speed: 50 to 500 rpm
Maximum jacket pressure
4.4 psi or 0.03 MPa
Drain valve Flush seal design with large opening and flat flange clamp
Agitator Style: impeller
Material: 304 stainless steel with PTFE liner
Condenser Dual-cooling coil design
Funnel Pressure equalizing
Vacuum gauge Mechanical
Swivel caster Four
Glass vessel temperature range
-110F to 400F
Vacuum level 20 torr
Vacuum sealing Glass or PTFE
Drain port ground clearance
12.5 inches
Reactor dimensions (WxDxH) 26 x 33 x 85"
Shipping dimensions 25 x 83 x 42"
Shipping weight 330 Lbs
Compliance ETL tested to UL and CSA standards
Standard Packages

R50-CC508-UDP6 Standard Package

 

 Part description

 Quantity

Part image

 Huber Unistat 405 -45C to +250C system
1 set  
 Huber adapters, tubing and fluid

  9256 x 2    90° Adaptor M24x1,5 female - M24x1,5 male
  9327 x 2    2m   (-60 to 260) - tubing
  9825 x 2    M24 X 1.5 (male) to 3/4" NPT
(male)
  6165 x 1    M60 (-60 to 115)   5L - fluid
  6166 x 2    M60 (-60 to 115) 10L - fluid

1 set  
 Jacketed glass vessel, lid, clamps and heavy duty stainless steel stand with casters (shipped pre-assembled)
1 set
 Glass vessel insulation jacket with openable viewing window 1 pc

 Vertical condenser with dual cooling coils, 2 chilling fluid ports and 1 vacuum port, glass

1 pc
 Glass condenser dispenser with drain port and PTFE open/close valve
1 set
 Glass material feeding funnel, lid, and PTFE open/close valve
1 set
 1" glass drain port with PTFE open/close valve
1 set
 Glass vacuum valve
1 set
 Stirring motor controller with material temperature display
1 pc
 Stirring motor and motor support
1 set  
 Mechanical vacuum gauge with two 3/8" hose barb ports
1 pc
 Temperature probe with PTFE seal
1 pc
 PTFE stirring blades, stainless steel rod with PTFE liner
1 pc
 Insulated hose with drain port & open/close valve x 2
 3/8" Stainless steel hose barb adapters x 2
4 pcs
 PTFE sealing tape 1 pc 
 PTFE stirring rod positioner/bearing kit
1 set
 Condenser dispenser connection kit 1 set
 Large opening material feeding port kit 1 set
 Bottom drain port sealing clamp  1 set
 Rubber-wrapped condenser dispenser support and condenser bracket 3 pcs
 Chilling fluid connector x 2, vacuum connector x 1
3 sets
 Allen key and backup inner hex screws 1 set
 Users manual 1 pc

 

Ulvac UDP-6 3/8 Accessories Package

 Part description

 Quantity

Part image

 ULVAC 220V UDP-6 6 cfm 6 torr 2-head diaphragm pump  and vacuum hose

 3/8 Accessories Package
 KF-38-1 x 1
 VH.10F x 1

 

1 set

 

KF25 wing nut flange quick clamp

1 pc

KF25 flange centering ring

1 pc

 Power Cord with plug (may be hardwired to unit or with a detachable plug) 1 PC

 

Huber Unistat 405 Package

 

 Part description

 Quantity

Part image

HUBER Unistat 405 -45°C to 250°C with Pilot ONE 1 pc

Mini-USB Cable 1 pc

E-Grade “Professional” (digital) 1 pc

Adaptor M16x1 male to M24x1.5 female 2 pc

             Huber adapters, tubing, and fluid

  9256 x 2    90° Adaptor M24x1,5 female -  M24x1,5 male
  9327 x 2    2m   (-60 to 260) - tubing
  9825 x 2    M24 X 1.5 (male) to 3/4" NPT (male)
  6165 x 1    M60 (-60 to 115)   5L - fluid
  6166 x 2    M60 (-60 to 115) 10L - fluid
1 set

 

User's manual 1 pc

Overview

Ai R-series single/dual jacketed glass reactors are designed for synthetic reaction of different types of materials in a controlled temperature and vacuum environment. Each reactor features adjustable stirring speeds and a constant pressure feeding funnel that allows you to add material to the vessel at a uniform and controlled speed. The built-in condenser makes it possible to recover some materials, also at a controlled rate of speed.

Features

  • Now includes a FREE high quality thermo insulation jacket (a $699 value) with open/close viewing window and top/bottom adjustable drawstrings, specially designed and made for Ai glass jacketed reactors. These jackets will extend chiller life, allow you to go down to a lower temperature, and also cut your utility bill.
  • Dual jacketed model allows you to draw vacuum from the outer jacket, thus protects your recirculating fluid temperature and gives you best control over your work. It also help prevents frost to form on the outside of the vessel, allowing you to see clearly into your material.
  • Solvent-resistant PTFE on all sealing components ensures long time durability and operation.
  • All glassware is hand-made from food grade high borosilicate glass that is heat/cold/corrosion-resistant.
  • Adjustable stirring rate provides great torque or high speed.
  • Patented PTFE stirring rod bearing for reliable and quiet operation.
  • Optional multi-layer stirring blades for optimal reaction results.
  • Wide range of temperature operations, from -110F to 400F.
  • Large condenser cooling surface for exceptional condensation performance.
  • Rugged stainless steel reinforced PTFE stirrer with anchored agitator, suitable for a wide range of viscous materials.
  • Easily visual operation with digital speed and temperature displays.
  • Heavy duty stainless steel supporting framework with lockable casters for mobility and stability. (whole support and glass vessel shipped pre-assembled)
  • One year warranty and lifetime US-based parts, service, and support.

Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

 

 

Copyright © 2008-2023 Across International. All rights reserved.